Information form customer:The average results for recovery are this. Lab Results SummaryTESTAlCaCdCoCuFeMgMnZnRecovRecovRecovRecovRecovRecovRecovRecovRecovExtractionDZ 988NE1 Aqua11,9%9,9%13,2%13,1%98,7%20,1%11,3%13,0%10,0%DZ 988NE2 Aqua13,4%12,0%13,2%-2,1%20,9%21,0%10,5%13,5%-1,1%DZ 988NE3 Aqua14,4%12,3%14,7%0,9%40,4%23,8%12,3%14,4%0,7%Extraction25%22%26%11%99%18%22%26%9%StrippingDZ 988NS1 Aqua0,0%0,0%0,0%0,0%0,3%0,0%0,0%0,0%3,1%DZ 988NS2 Aqua0,0%0,0%0,0%0,0%0,1%0,1%0,0%0,0%0,0%No tripped0,0%0,0%0,0%0%0%0%0%0%0% We are happy with the copper recovery and stripping efficiency. Where we find a problem is in the differences of extraction of other metals. DZ988N/Acorga M5604AlCaCdCoCuFeMgMnZnRecovRecovRecovRecovRecovRecovRecovRecovRecovExctraction5%6%6%2%0%9%4%6%3%Stripping0%0%0%0%0%0%0%0%0% Here you have the increase of extraction of different metals. We are really concern about the extraction of 2% more Cobalt (losses in the cobalt circuit) 9% of iron and a 3% of Zn hat will interfere with the optimal parameters of the EW circuit.The working conditions have been.EXTRACTION:E1 pH 1.2- 40°CE2 PH 1.3-40°CE3 pH 1.5-40°C(in the factory we lose 1.5 C degrees between E3 and E1) STRIPPING：S1 pH 0.5S2 PH 0.25 20% Extractant, Ratio Organic/Aqua 2.5 in extraction and 0.5 in Stripping The reagents used for pH adjustment where, NaOH solution and H2SO4 Solution.In the stripping circuit we look to use parameters that we will use in the EW circuit for an optimal copper recovery stage.Mr. Jeven, we are thinking to work more with your product in the future, looking to optimize temperature pH, Extractant load (x%) etc. But I want some advice from you. Please check the results and share with me your observations. Our suggestion:Copper extractant specialist:Please use DZ988N to extract copper as clean as possible, the pH value should be between 2.2 to 2.5, the extraction effect will be best. After that, the cost in process of zinc, cobalt extraction and the removal of impurities will be cheaper.For DZ988N also need notice two points: the working temperature can be nature temperature, the volume rate of organic/aqua should be 1:1, if the content of copper is very high, can use 2:1. On our catalog has introduced this laboratory test process clearly, please refer it. Professor of Product Development and Applications:1. Extract Cu: As your data, the extraction ability is too strong, all metal was extracted out, especially Cu & Fe, lost the selective ability. So, please adjust the concentrate of organic phase to 10%-15%, at normal temperature, use 1:1 phase ratio, repeat to test it, till reach the selective ability of Cu:Fe over 1000:1, it means that only extract Cu out. If the content of Cu is high, can raise the phase ratio of organic and aqueous, until 2:1.2. Remove impurity by precipitation: Use NaOH, PH value 3.8-4.2.3. Use P204 remove impurity: Use 260# solvent oil dilute the concentrate to 10%, can adjust the phase ratio, to remove Fe, Zn, Al and Mg.4. Use DZ272 around 50°C temperature to extract Co, Mg out, leave Ni. Mg can be washed away. After getting our suggestion, customer said: Dear Jeven, we are finishing some test. We will repeat yours when we finish our actual lab program following your indications. Let wait for their result.
Nickel Extraction ReagentDZ272COMPONENTS：Bis-(2,4,4-Trimethylpentyl)-Phosphinic Acid The content of Bis-(2,4,4-Trimethylpentyl)-Phosphinic Acid more than 95%.Colorless or near colorless liquid, light fruity, faintly acid, nontoxic, there is not corrosion property for most steel plastic container. DANGEROUS UN3082 Prevention ◆Smoking, eating and drinking should be prohibited in the application area.◆Provide sufficient air exchange and /or exhaust in work rooms.◆Dispose of rinse water in accordance with local and national regulation.◆Keep away from open flames, hot surfaces and sources of ignition. EmergencyResponse◆Use personal protective equipment. Ensure adequate ventilation.◆Prevent product from entering drains. Prevent further leakage or spillage if safe to do so. If the product contaminates rivers and lakes or drains inform respective authorities.◆Contain spillage, and then collect with non-combustible absorbent material. (as sand, earth, diatomaceous earth, vermiculite) and place in container for disposal according to local/national regulations). Keep in suitable, closed containers for disposal. Storage◆No smoking.◆Keep container tightly closed in a dry and well-ventilated place.◆Containers which are opened must be carefully resealed and kept upright to prevent leakage.◆Electrical installations/working materials must completely with the technological safety standards.Environmental Precautions◆Prevent this material release to the environment such as ground water, sewage system, household garbage etc. without proper governmental permits.Disposal◆Send to a licensed waste management company.Please refer to the Material Safety Data Sheet Emergency phone number: +86-18937129559
Copper Extraction ReagentDZ988NCOMPONENTS：Oxime mixture (5-nonyl salicylic aldoxime&2-hydroxy-5-nonyl acetophenone oxime, 50% Distillates (petroleum), hydrotreated light 50%)flammable liquid, its vapour or fog is irritant to eyes, mucosa, respiratory tract, and in case of open fire, high heat causes combustion & explosion. DANGEROUS UN3082 Prevention ◆Store in a well-ventilated area, keep container tightly closed.◆Obey operation rules strictly.◆Operator must wear full-face respirator with multi-purpose combination(US), tightly fitting safety goggles and antistatic clothing.◆Keep away from heat, hot surfaces, sparks, open flame and other ignition sources. Smoking and cellphone are forbidden in workplace.◆Use explosion resistant ventilating devices. EmergencyResponse◆Isolation polluted area, strictly limited access.◆Emergency personnel wear positive pressure self-contained breathing apparatus. Wear chemical impermeable clothing and gloves.◆Remove all sources of ignition, cut off the source of leakage.◆Slight leakage: absorb spilled material in dry sand or inert absorbent.◆Large amount of leakage: contain a spill by bund, cover with anti-dissolution foam, reduce evaporation. Transfer with anti-explosion pump to tanker. recycling or shipped to the specific waste disposal sites. Storage◆Keep container in a dry, cool and well-ventilated place.◆Keep away from heat/sparks/open flames/sunlight.◆Keep containers tightly sealed，prevent damp.◆Store away from oxidant and other incompatible materials.Environmental Precautions◆Prevent wastewater into confined space, and the water environment such as the sewer , drainage ditch. Disposal ◆Dispose with well controlled incinerationPlease refer to the Material Safety Data Sheet Emergency phone number:+86-18937129559
Customer's has three kinds of material, first one is the concentrate of laterite ore, second and third are wasted battery liquid:Item No.SpcificationNiCoMnZnCaFeAlSiCuMg1Processed ore382.94.8210.150.360.3184.108.40.206Waste battery liquid 16.6415.64.8620.314.363Waste battery liquid 210.9114.9910.320.979.821.68First. Use P204 to remove the impurities, only left Nickel and Cobalt ion. Second. Saponify the liquid to 45%, keep temperature to around 50°C. Third. As the components and content of ore, we suggest to use below extraction process: Item No.1: Dilute DZ272 to 15%-20%, use Organic phase with Aqueous phase to 1:1, use 3 to 5 steps extraction process to get the nickel ion, use 1 mol (98%) sulfuric acid for reverse extraction to get pure nickel sulfate. Item No.2: Dilute DZ272 to 15%-20%, use Organic phase with Aqueous phase to 2:1, use 3 to 5 steps extraction process to get the nickel, then use 1 mol (98%) sulfuric acid for reverse extraction to get pure nickel sulfate. Item No.2: Dilute DZ272 to 20%, use Organic phase with Aqueous phase to 2:1 or 3:1, use 3 to 5 steps extraction process to get the nickel ion, use 1 mol (98%) sulfuric acid for reverse extraction to get pure nickel sulfate.If you have this ore and want to use our extractant to extract it, please tell us the detailed analysis report, we can give you the technical proposal for your material. Please write email to firstname.lastname@example.org.